还原棕R
还原棕R用途
还原棕 R 主要用于棉纤维的染色，匀染性很好，亲和力也好。还用于涤棉、涤黏、维棉等混纺织物的染色，涤纶组分有轻微沾色。可与分散染料同浴热熔法染色，也可两浴法染色。还可与还原棕 G、还原棕 GG、还原棕 BR 等拼染深浅色光各异的棕色，也用于制备有机颜料。
还原棕R名称
[ CAS 号 ]:
131-92-0
[ 中文名 ]:
还原棕R
[ 英文名 ]:
Vat Brown 3
[中文别名 ]:
[英文别名 ]:
- Tinon Brown GRF
- Tinon Brown GR
- Caledon Brown R
- Calcoloid Brown R
- Novatic Brown R
- vat brown R
- Vat Brown 3
- Ahcovat Brown AR
- Benzadone Brown R
- Vat Brown K
还原棕R物理化学性质
[ 密度 ]:
1.537
[ 沸点 ]:
685.54°C (rough estimate)
[ 熔点 ]:
180ºC
[ 分子式 ]:
C42H23N3O6
[ 分子量 ]:
665.64900
[ 精确质量 ]:
665.15900
[ PSA ]:
142.27000
[ LogP ]:
7.52250
[ 外观性状 ]:
无气味的棕色至暗棕色粉末
[ 折射率 ]:
1.831
还原棕R毒性和生态
CHEMICAL IDENTIFICATION
- RTECS NUMBER :
- CV5857000
- CAS REGISTRY NUMBER :
- 131-92-0
- BEILSTEIN REFERENCE NO. :
- 0382039
- LAST UPDATED :
- 199710
- DATA ITEMS CITED :
- 8
- MOLECULAR FORMULA :
- C42-H23-N3-O6
HEALTH HAZARD DATA
ACUTE TOXICITY DATA
- TYPE OF TEST :
- LD50 - Lethal dose, 50 percent kill
- ROUTE OF EXPOSURE :
- Oral
- SPECIES OBSERVED :
- Rodent - rat
- DOSE/DURATION :
- >6 gm/kg
- TOXIC EFFECTS :
- Details of toxic effects not reported other than lethal dose value
- REFERENCE :
- GISAAA Gigiena i Sanitariya. For English translation, see HYSAAV. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1936- Volume(issue)/page/year: 52(6),85,1987
- TYPE OF TEST :
- LD50 - Lethal dose, 50 percent kill
- ROUTE OF EXPOSURE :
- Intraperitoneal
- SPECIES OBSERVED :
- Rodent - rat
- DOSE/DURATION :
- 1410 mg/kg
- TOXIC EFFECTS :
- Sense Organs and Special Senses (Olfaction) - effect, not otherwise specified Behavioral - food intake (animal) Behavioral - aggression
- REFERENCE :
- GISAAA Gigiena i Sanitariya. For English translation, see HYSAAV. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1936- Volume(issue)/page/year: 52(6),85,1987
- TYPE OF TEST :
- LD50 - Lethal dose, 50 percent kill
- ROUTE OF EXPOSURE :
- Oral
- SPECIES OBSERVED :
- Rodent - mouse
- DOSE/DURATION :
- >6 gm/kg
- TOXIC EFFECTS :
- Details of toxic effects not reported other than lethal dose value
- REFERENCE :
- GISAAA Gigiena i Sanitariya. For English translation, see HYSAAV. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1936- Volume(issue)/page/year: 52(6),85,1987
- TYPE OF TEST :
- LD50 - Lethal dose, 50 percent kill
- ROUTE OF EXPOSURE :
- Intraperitoneal
- SPECIES OBSERVED :
- Rodent - mouse
- DOSE/DURATION :
- 3600 mg/kg
- TOXIC EFFECTS :
- Sense Organs and Special Senses (Olfaction) - effect, not otherwise specified Behavioral - food intake (animal) Behavioral - aggression
- REFERENCE :
- GISAAA Gigiena i Sanitariya. For English translation, see HYSAAV. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1936- Volume(issue)/page/year: 52(6),85,1987 ** OTHER MULTIPLE DOSE TOXICITY DATA **
- TYPE OF TEST :
- TDLo - Lowest published toxic dose
- ROUTE OF EXPOSURE :
- Oral
- SPECIES OBSERVED :
- Rodent - rat
- DOSE/DURATION :
- 60 gm/kg/30D-I
- TOXIC EFFECTS :
- Liver - changes in liver weight Kidney, Ureter, Bladder - other changes Blood - pigmented or nucleated red blood cells
- REFERENCE :
- GISAAA Gigiena i Sanitariya. For English translation, see HYSAAV. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1- 1936- Volume(issue)/page/year: 52(6),85,1987 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - M3094 No. of Facilities: 56 (estimated) No. of Industries: 1 No. of Occupations: 7 No. of Employees: 4491 (estimated) No. of Female Employees: 3930 (estimated)
还原棕R合成路线
还原棕R上下游产品
还原棕R上游产品
还原棕R下游产品
还原棕R制备
以 1-溴-4-苯甲酰氨基蒽醌和 1-氨基-5-苯甲酰氨基蒽醌为原料，首先将两者在无水乙酸钠存在下缩合，用发烟硫酸环化，经次氯酸钠氧化即得产物。经过滤、粉碎、干燥得成品。
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