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1-氮杂环辛-2-酮

1-氮杂环辛-2-酮用途

该品为药物胍乙啶的中间体。

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1-氮杂环辛-2-酮名称

[ CAS 号 ]:
673-66-5

[ 中文名 ]:
氮杂环辛酮

[ 英文名 ]:
2-Azocanone

[中文别名 ]:

[英文别名 ]:

2-Azocanone
MFCD00003271
2-Azocinol, 3,4,5,6,7,8-hexahydro-, (1E)-
Azocan-2-on
EINECS 211-611-9
(1E)-3,4,5,6,7,8-Hexahydro-2-azocinol
2(1H)-Azocinone, hexahydro-
Azocan-2-one

1-氮杂环辛-2-酮物理化学性质

[ 密度 ]:
0.9±0.1 g/cm3

[ 沸点 ]:
287.6±0.0 °C at 760 mmHg

[ 熔点 ]:
35-38 °C(lit.)

[ 分子式 ]:
C₇H₁₃NO

[ 分子量 ]:
127.184

[ 闪点 ]:
143.3±3.4 °C

[ 精确质量 ]:
127.099716

[ PSA ]:
29.10000

[ LogP ]:
0.24

[ 外观性状 ]:
白色至棕色结晶粉末

[ 蒸汽压 ]:
0.0±0.6 mmHg at 25°C

[ 折射率 ]:
1.445

[ 储存条件 ]:
存放于惰性气体之中;避免湿气 (吸湿)

1-氮杂环辛-2-酮MSDS

1-氮杂环辛-2-酮毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: CN4810000

CHEMICAL NAME :: 2(1H)-Azocinone, hexahydro-

CAS REGISTRY NUMBER :: 673-66-5

BEILSTEIN REFERENCE NO. :: 0108987

LAST UPDATED :: 199612

DATA ITEMS CITED :: 2

MOLECULAR FORMULA :: C7-H13-N-O

MOLECULAR WEIGHT :: 127.21

WISWESSER LINE NOTATION :: T8MVTJ

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 270 mg/kg

TOXIC EFFECTS :: Behavioral - convulsions or effect on seizure threshold Behavioral - analgesia

REFERENCE :: JPMSAE Journal of Pharmaceutical Sciences. (American Pharmaceutical Assoc., 2215 Constitution Ave., NW, Washington, DC 20037) V.50- 1961- Volume(issue)/page/year: 60,1058,1971

TYPE OF TEST :: LDLo - Lowest published lethal dose

ROUTE OF EXPOSURE :: Subcutaneous

SPECIES OBSERVED :: Amphibian - frog

DOSE/DURATION :: 250 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: AEXPBL Archiv fuer Experimentelle Pathologie und Pharmakologie. (Leipzig, Ger. Dem. Rep.) V.1-109, 1873-1925. For publisher information, see NSAPCC. Volume(issue)/page/year: 50,199,1903

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1-氮杂环辛-2-酮安全信息

[ 符号 ]:

GHS07

[ 信号词 ]:
Warning

[ 危害声明 ]:
H302

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xn: Harmful;

[ 风险声明 (欧洲) ]:
R22

[ 安全声明 (欧洲) ]:
S24/25

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ RTECS号 ]:
CN4810000

[ 海关编码 ]:
2933790090

1-氮杂环辛-2-酮合成路线

1-氮杂环辛-2-酮上下游产品

1-氮杂环辛-2-酮上游产品

1-氮杂环辛-2-酮下游产品

1-氮杂环辛-2-酮制备

由环庚酮经肟化、重排而得。将硫酸、硫酸羟胺抽入干燥的反应锅内，加热搅拌溶解，在110-120℃缓缓加入环庚酮。加完后保温搅拌1.5h，降温至70-80℃。趁热放料至碎冰中，加氢氧化钠溶液至pH为14。用氯仿萃取，萃取液蒸馏回收氯仿后进行减压蒸馏，收集140℃（2.0kPa）馏分，得庚内酰胺。

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1-氮杂环辛-2-酮海关

[ 海关编码 ]: 2933790090

[ 中文概述 ]:
2933790090 其他内酰胺. 增值税率:17.0% 退税率:9.0% 监管条件:无最惠国关税:9.0% 普通关税:20.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 乌洛托品请注明外观, 6－己内酰胺请注明外观, 签约日期

[ Summary ]:
2933790090. other lactams. VAT:17.0%. Tax rebate rate:9.0%. . MFN tariff:9.0%. General tariff:20.0%

1-氮杂环辛-2-酮文献

Gravity, a regulation factor in the differentiation of rat bone marrow mesenchymal stem cells.

J. Biomed. Sci. 16 , 87, (2009)

Stem cell therapy has emerged as a potential therapeutic option for tissue engineering and regenerative medicine, but many issues remain to be resolved, such as the amount of seed cells, committed dif...

Enhancement of ninhydrin- or DFO-treated latent fingerprints on thermal paper.

J. Forensic Sci. 52 , 649-655, (2007)

A new method for enhancement of ninhydrin or 1,8-diazafluoren-9-one (DFO)-treated latent fingerprints on thermal paper will be described. Most thermosensitive surfaces of thermal paper become dark whe...

Conformational energy studies of the growth hormone inhibitor, cyclo (Aha-Cys-Phe-D-Trp-Lys-Thr-Cys).

Biochem. Biophys. Res. Commun. 95(1) , 61-6, (1980)

更多文献

1-氮杂环辛-2-酮

1-氮杂环辛-2-酮用途

1-氮杂环辛-2-酮名称

1-氮杂环辛-2-酮物理化学性质

1-氮杂环辛-2-酮MSDS

详细MSDS(安全技术说明书)

1-氮杂环辛-2-酮毒性和生态

CHEMICAL IDENTIFICATION

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

1-氮杂环辛-2-酮安全信息

1-氮杂环辛-2-酮合成路线

详细合成路线

1-氮杂环辛-2-酮上下游产品

1-氮杂环辛-2-酮上游产品

1-氮杂环辛-2-酮下游产品

1-氮杂环辛-2-酮制备

1-氮杂环辛-2-酮海关

1-氮杂环辛-2-酮文献

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