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4,7-二甲氧基-1,10-菲咯啉

4,7-二甲氧基-1,10-菲咯啉名称

[ CAS 号 ]:
92149-07-0

[ 中文名 ]:
4,7-二甲氧基-1,10-菲咯啉

[ 英文名 ]:
4,7-Dimethoxy-1,10-phenanthroline

[中文别名 ]:

4,7-二甲氧基-1,10-菲罗啉

[英文别名 ]:

1,10-Phenanthroline, 4,7-dimethoxy-
4,7-Dimethoxy-1,10-phenanthroline

4,7-二甲氧基-1,10-菲咯啉物理化学性质

[ 密度 ]:
1.3±0.1 g/cm3

[ 沸点 ]:
373.1±37.0 °C at 760 mmHg

[ 熔点 ]:
197-212ºC

[ 分子式 ]:
C₁₄H₁₂N₂O₂

[ 分子量 ]:
240.257

[ 闪点 ]:
135.9±16.8 °C

[ 精确质量 ]:
240.089874

[ PSA ]:
44.24000

[ LogP ]:
2.31

[ 外观性状 ]:
固体;White to Gray to Brown powder to crystal

[ 蒸汽压 ]:
0.0±0.8 mmHg at 25°C

[ 折射率 ]:
1.667

[ 储存条件 ]:
存放于惰性气体之中;避免空气

4,7-二甲氧基-1,10-菲咯啉MSDS

4,7-二甲氧基-1,10-菲咯啉安全信息

[ 符号 ]:

GHS05, GHS07, GHS09

[ 信号词 ]:
Danger

[ 危害声明 ]:
H302-H318-H400

[ 警示性声明 ]:
P273-P280-P305 + P351 + P338

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xn: Harmful;N: Dangerous for the environment;

[ 风险声明 (欧洲) ]:
22-41-50

[ 安全声明 (欧洲) ]:
26-39-61

[ 危险品运输编码 ]:
UN 3077 9/PG 3

[ 海关编码 ]:
2933990090

4,7-二甲氧基-1,10-菲咯啉合成路线

4,7-二甲氧基-1,10-菲咯啉上下游产品

4,7-二甲氧基-1,10-菲咯啉上游产品

4,7-二甲氧基-1,10-菲咯啉下游产品

4,7-二甲氧基-1,10-菲咯啉海关

[ 海关编码 ]: 2933990090

[ 中文概述 ]:
2933990090. 其他仅含氮杂原子的杂环化合物. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:6.5%. 普通关税:20.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 乌洛托品请注明外观, 6－己内酰胺请注明外观, 签约日期

[ Summary ]:
2933990090. heterocyclic compounds with nitrogen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

4,7-二甲氧基-1,10-菲咯啉文献

4,7-Dimethoxy-1,10-phenanthroline: an excellent ligand for the Cu-catalyzed N-arylation of imidazoles.

Org. Lett. 8 , 2779, (2006)

[reaction: see text] 4,7-Dimethoxy-1,10-phenanthroline (L) was found to be an efficient ligand for the copper-catalyzed N-arylation of imidazole with aryl iodides and bromides under mild conditions. A...

Copper-catalyzed N-arylation of imidazoles and benzimidazoles.

J. Org. Chem. 72 , 6190, (2007)

4,7-Dimethoxy-1,10-phenanthroline (L1c) was found to be an efficient ligand for the copper-catalyzed N-arylation of imidazoles and benzimidazoles with both aryl iodides and bromides under mild conditi...

A general and efficient copper catalyst for the amidation of aryl halides.

J. Am. Chem. Soc. 124 , 7421, (2002)

An experimentally simple and inexpensive catalyst system was developed for the amidation of aryl halides by using 0.2-10 mol % of CuI, 5-20 mol % of a 1,2-diamine ligand, and K(3)PO(4), K(2)CO(3), or ...

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