Catalyzed metalation applied to 2-methoxypyridine

F Trécourt, M Mallet, F Marsais…

Index: Journal of Organic Chemistry, , vol. 53, # 7 p. 1367 - 1371

Full Text: HTML

Citation Number: 60

Abstract

... Chem., Vol. ... The organic layer was dried over anhydrous mag- nesium sulfate (MgS04), concentrated, and then distilled. ... 2). Pure 2 was ob- tained by vacuum distillation to afford a colorless liquid: bp 55 "C (3 Torr); 'H NMR 6 0.25 (s, 9 H), 3.9 (s, 3 H), 6.75 [dd, 1 H, J = 7.0 Hz ...