Journal of the Chinese Chemical Society

One pot preparation of amides from azo compounds by Sm/TiCl4

X Li, YM Zhang

Index: Li, Xue; Zhang, Yong-Min Journal of the Chinese Chemical Society, 2005 , vol. 52, # 6 p. 1219 - 1222

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Abstract

Azo compounds were conveniently reduced by a system consisting of Sm/TiCl4 to produce aniline an- ions. This anion species reacted smoothly with aliphatic acyl chlorides or acid anhydrides to afford corre- sponding amides under mild and neutral conditions. ... Keywords: Amides; Azo compound; Sm/TiCl4; Reduction. ... Amides are important commercial and biological com- pounds. Because amides constitute the backbone of protein molecules, their chemistry is ...

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