Tetrahedron

Comparisons of O-acylation and Friedel–Crafts acylation of phenols and acyl chlorides and Fries rearrangement of phenyl esters in trifluoromethanesulfonic acid: …

R Murashige, Y Hayashi, S Ohmori, A Torii, Y Aizu…

Index: Tetrahedron, , vol. 67, # 3 p. 641 - 649

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Citation Number: 32

Abstract

... Please enable JavaScript to use all the features on this page. Tetrahedron. Volume 67, Issue 3, 21 January 2011, Pages 641–649. Cover image Cover image. ... Scheme 5. Homotyrosine synthesis with Friedel–Crafts acylation and Fries rearrangement. (i) 3% TfOH, CH 3 CN, room ...

 Related Synthetic Route
3-Methylphenol acetate Structure

122-46-3

3-Methylphenol ...

~62%

2'-Hydroxy-4'-methylacetophenone Structure

6921-64-8

2'-Hydroxy-4'-m...

4′-Hydroxy-2′-methylacetophenone Structure

875-59-2

4′-Hydroxy-2′-m...

m-Cresol Structure

108-39-4

m-Cresol

~%

2'-Hydroxy-4'-methylacetophenone Structure

6921-64-8

2'-Hydroxy-4'-m...

4′-Hydroxy-2′-methylacetophenone Structure

875-59-2

4′-Hydroxy-2′-m...

3-Methylphenol acetate Structure

122-46-3

3-Methylphenol ...

~31%

2'-Hydroxy-4'-methylacetophenone Structure

6921-64-8

2'-Hydroxy-4'-m...

4′-Hydroxy-2′-methylacetophenone Structure

875-59-2

4′-Hydroxy-2′-m...

m-Cresol Structure

108-39-4

m-Cresol

~%

2'-Hydroxy-4'-methylacetophenone Structure

6921-64-8

2'-Hydroxy-4'-m...

4′-Hydroxy-2′-methylacetophenone Structure

875-59-2

4′-Hydroxy-2′-m...

Butyryl chloride Structure

141-75-3

Butyryl chloride

Phenol Structure

108-95-2

Phenol

~10%

1-(4-Hydroxyphenyl)butan-1-one Structure

1009-11-6

1-(4-Hydroxyphe...

Acetyl chloride Structure

75-36-5

Acetyl chloride

2-Naphthol Structure

135-19-3

2-Naphthol

~53%

1-(2-hydroxy-1-naphthyl)ethan-1-one Structure

574-19-6

1-(2-hydroxy-1-...

1-(3-hydroxynaphthalen-2-yl)ethanone Structure

17056-93-8

1-(3-hydroxynap...

Valeryl chloride Structure

638-29-9

Valeryl chloride

Phenol Structure

108-95-2

Phenol

~98%

4'-Hydroxyvalerophenone Structure

2589-71-1

4'-Hydroxyvaler...

1-Naphthalenol Structure

90-15-3

1-Naphthalenol

Acetyl chloride Structure

75-36-5

Acetyl chloride

~26%

2-Acetyl-1-naphthol Structure

711-79-5

2-Acetyl-1-naphthol

Ethanone,1-(4-hydroxy-1-naphthalenyl)- Structure

3669-52-1

Ethanone,1-(4-h...

4-Fluorophenyl acetate Structure

405-51-6

4-Fluorophenyl ...

~93%

5′-Fluoro-2′-hydroxyacetophenone Structure

394-32-1

5′-Fluoro-2′-hy...


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