Acetamide,2-chloro-N-(4-methoxyphenyl)-

Modify Date: 2024-01-10 01:46:10

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure
Acetamide,2-chloro-N-(4-methoxyphenyl)- structure
 Common Name Acetamide,2-chloro-N-(4-methoxyphenyl)-
CAS Number 22303-36-2 Molecular Weight 199.63400
Density 1.264 g/cm3 Boiling Point 378.5ºC at 760 mmHg
Molecular Formula C9H10ClNO2 Melting Point 121-122ºC
MSDS N/A Flash Point 182.7ºC

 Names

Name 2-chloro-N-(4-methoxyphenyl)acetamide
Synonym More Synonyms

 Chemical & Physical Properties

Density 1.264 g/cm3
Boiling Point 378.5ºC at 760 mmHg
Melting Point 121-122ºC
Molecular Formula C9H10ClNO2
Molecular Weight 199.63400
Flash Point 182.7ºC
Exact Mass 199.04000
PSA 38.33000
LogP 1.94550
Vapour Pressure 6.26E-06mmHg at 25°C
Index of Refraction 1.573

 Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
AE8295000
CHEMICAL NAME :
p-Acetanisidide, 2-chloro-
CAS REGISTRY NUMBER :
22303-36-2
BEILSTEIN REFERENCE NO. :
0779019
LAST UPDATED :
199612
DATA ITEMS CITED :
1
MOLECULAR FORMULA :
C9-H10-Cl-N-O2
MOLECULAR WEIGHT :
199.65
WISWESSER LINE NOTATION :
G1VMR DO1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Intravenous
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
110 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) Volume(issue)/page/year: NX#02937

 Safety Information

Hazard Codes Xi: Irritant;
HS Code 2924299090

 Synthetic Route

p-Anisidine structure

p-Anisidine

CAS#:104-94-9

Chloroacetyl chloride structure

Chloroacetyl ch...

CAS#:79-04-9

~99%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: Ma, Liang; Li, Shilin; Zheng, Hao; Chen, Jinying; Lin, Lin; Ye, Xia; Chen, Zhizhi; Xu, Qinyuan; Chen, Tao; Yang, Jincheng; Qiu, Neng; Wang, Guangcheng; Peng, Aihua; Ding, Yi; Wei, Yuquan; Chen, Lijuan European Journal of Medicinal Chemistry, 2011 , vol. 46, # 6 p. 2003 - 2010
p-Anisidine structure

p-Anisidine

CAS#:104-94-9

Chloroacetic acid structure

Chloroacetic acid

CAS#:79-11-8

~19%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: N30 PHARMACEUTICALS, LLC; SUN, Xicheng; QIU, Jian; STOUT, Adam Patent: WO2012/83165 A1, 2012 ; Location in patent: Page/Page column 92 ;
4-Methoxybenzaldehyde structure

4-Methoxybenzal...

CAS#:123-11-5

Chloroacetyl chloride structure

Chloroacetyl ch...

CAS#:79-04-9

~%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: European Journal of Medicinal Chemistry, , vol. 46, # 3 p. 835 - 844
(2,4-difluorobenzylidene)(4-methoxyphenyl)amine structure

(2,4-difluorobe...

CAS#:302931-51-7

Chloroacetyl chloride structure

Chloroacetyl ch...

CAS#:79-04-9

~17%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: Elriati, Ali; Loose, Jutta; Mayrhofer, Roswitha; Bergmann, Hans-Joachim; Otto, Hans-Hartwig Monatshefte fur Chemie, 2008 , vol. 139, # 7 p. 835 - 846
p-Anisidine structure

p-Anisidine

CAS#:104-94-9

~%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: Tetrahedron, , vol. 54, # 38 p. 11501 - 11516
tert-butyl(1-(4-methoxyphenyl)vinyloxy)dimethylsilane structure

tert-butyl(1-(4...

CAS#:80676-78-4

~%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: Journal of the Chemical Society, Chemical Communications, , p. 1727 - 1728
p-Anisidine structure

p-Anisidine

CAS#:104-94-9

Chloroacetic anhydride structure

Chloroacetic an...

CAS#:541-88-8

~%

Acetamide,2-chloro-N-(4-methoxyphenyl)- Structure

Acetamide,2-chl...

CAS#:22303-36-2

Literature: Rahaim Jr., Ronald J.; Maleczka Jr., Robert E. Synthesis, 2006 , # 19 p. 3316 - 3340

 Customs

HS Code 2924299090
Summary 2924299090. other cyclic amides (including cyclic carbamates) and their derivatives; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

 Synonyms

p-ACETANISIDIDE,2-CHLORO
2-Chloro-p-acetanisidide
2-chloro-4-methoxyacetanilide
MFCD00018907
2-CHLORO-PARA-ACETANISIDIDE
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