4-nitrobenzenesulfenyl chloride
4-nitrobenzenesulfenyl chloride structure
|
Common Name | 4-nitrobenzenesulfenyl chloride | ||
|---|---|---|---|---|
| CAS Number | 937-32-6 | Molecular Weight | 189.61900 | |
| Density | 1.492 (estimate) | Boiling Point | 125 °C0.1 mm Hg(lit.) | |
| Molecular Formula | C6H4ClNO2S | Melting Point | 48-51 ℃(lit.) | |
| MSDS | Chinese USA | Flash Point | >230 °F | |
| Symbol |
GHS05 |
Signal Word | Danger | |
| Name | (4-nitrophenyl) thiohypochlorite |
|---|---|
| Synonym | More Synonyms |
| Density | 1.492 (estimate) |
|---|---|
| Boiling Point | 125 °C0.1 mm Hg(lit.) |
| Melting Point | 48-51 ℃(lit.) |
| Molecular Formula | C6H4ClNO2S |
| Molecular Weight | 189.61900 |
| Flash Point | >230 °F |
| Exact Mass | 188.96500 |
| PSA | 71.12000 |
| LogP | 3.36390 |
| Appearance of Characters | solid |
| Index of Refraction | 1.6000 (estimate) |
| Storage condition | 2-8°C |
| Symbol |
GHS05 |
|---|---|
| Signal Word | Danger |
| Hazard Statements | H314 |
| Precautionary Statements | P280-P305 + P351 + P338-P310 |
| Personal Protective Equipment | Eyeshields;Faceshields;full-face particle respirator type N100 (US);Gloves;respirator cartridge type N100 (US);type P1 (EN143) respirator filter;type P3 (EN 143) respirator cartridges |
| Hazard Codes | C |
| Risk Phrases | 34 |
| Safety Phrases | 26-27-28-36/37/39-45 |
| RIDADR | UN 3261 8/PG 2 |
| WGK Germany | 3 |
| Packaging Group | III |
| HS Code | 2930909090 |
|
~97%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Johnston,M.; Raines,R.; Walsh,C. Journal of the American Chemical Society, 1980 , vol. 102, p. 4241 |
|
~99%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Petrovic, Goran; Cekovic, Zivorad Synthesis, 2004 , # 10 p. 1671 - 1679 |
|
~71%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V. Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880 Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163 |
|
~%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Thea, Sergio; Cevasco, Giorgio Tetrahedron Letters, 1988 , vol. 29, # 23 p. 2865 - 2866 |
|
~70%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Levchenko, E. S.; Pel'kis, N. P.; Kalinin, V. N.; Duzhak, A. A. Journal of Organic Chemistry USSR (English Translation), 1982 , p. 1028 - 1033 Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1191 - 1197 |
|
~%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Zincke; Lenhardt Justus Liebigs Annalen der Chemie, 1913 , vol. 400, p. 9 |
|
~%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Dubinina,T.N.; Levchenko,E.S. Journal of Organic Chemistry USSR (English Translation), 1979 , vol. 15, p. 660 - 664 Zhurnal Organicheskoi Khimii, 1979 , vol. 15, p. 743 - 748 |
|
~%
4-nitrobenzenes... CAS#:937-32-6
Detail
|
| Literature: Billman; O'Mahony Journal of the American Chemical Society, 1939 , vol. 61, p. 2340 |
|
~%
4-nitrobenzenes... CAS#:937-32-6 |
| Literature: Zincke; Lenhardt Justus Liebigs Annalen der Chemie, 1913 , vol. 400, p. 9 |
| Precursor 9 | |
|---|---|
| DownStream 10 | |
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CAS#:27691-43-6| HS Code | 2930909090 |
|---|---|
| Summary | 2930909090. other organo-sulphur compounds. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0% |
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A novel synthetic route to 3-sulfenyl- and 3-selenylindoles by n-Bu4NI-induced electrophilic cyclization.
Org. Lett. 11(1) , 173-6, (2009) 3-Sulfenyl- and 3-selenylindoles are prepared in excellent yields by the palladium/copper-catalyzed crossing coupling of N,N-dialkyl-o-iodoanilines and terminal alkynes, followed by electrophilic cycl... |
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