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1,5,6,7-四氢-4H-吲哚-4-酮

1,5,6,7-四氢-4H-吲哚-4-酮用途

心得静的中间体。

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1,5,6,7-四氢-4H-吲哚-4-酮名称

[ CAS 号 ]:
13754-86-4

[ 中文名 ]:
1,5,6,7-四氢-4H-吲哚-4-酮

[ 英文名 ]:
1,5,6,7-Tetrahydro-4H-indol-4-one

[中文别名 ]:

4-氧代-1,5,6,7-四氢吲哚

[英文别名 ]:

4,5,6,7-Tetrahydro-4-oxoindole
6,7-Dihydro-1H-indol-4(5H)-one
1,5,6,7-Tetrahydro-4H-indol-4-one
4-Oxo-4,5,6,7-tetrahydroindole
MFCD00075438

1,5,6,7-四氢-4H-吲哚-4-酮物理化学性质

[ 密度 ]:
1.2±0.1 g/cm3

[ 沸点 ]:
310.6±11.0 °C at 760 mmHg

[ 熔点 ]:
188-190 °C(lit.)

[ 分子式 ]:
C₈H₉NO

[ 分子量 ]:
135.163

[ 闪点 ]:
149.6±26.7 °C

[ 精确质量 ]:
135.068420

[ PSA ]:
32.86000

[ LogP ]:
1.14

[ 外观性状 ]:
固体;White to Light yellow to Light orange powder to crystal

[ 蒸汽压 ]:
0.0±0.7 mmHg at 25°C

[ 折射率 ]:
1.592

[ 储存条件 ]:
室温，干燥

1,5,6,7-四氢-4H-吲哚-4-酮MSDS

详细MSDS(安全技术说明书)

1,5,6,7-四氢-4H-吲哚-4-酮安全信息

[ 符号 ]:

GHS07

[ 信号词 ]:
Warning

[ 危害声明 ]:
H315-H319-H335

[ 警示性声明 ]:
P261-P305 + P351 + P338

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xi: Irritant;

[ 风险声明 (欧洲) ]:
R36/37/38

[ 安全声明 (欧洲) ]:
S26-S37/39

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ 海关编码 ]:
2933990090

1,5,6,7-四氢-4H-吲哚-4-酮合成路线

详细合成路线

1,5,6,7-四氢-4H-吲哚-4-酮上下游产品

1,5,6,7-四氢-4H-吲哚-4-酮上游产品

1,5,6,7-四氢-4H-吲哚-4-酮下游产品

1,5,6,7-四氢-4H-吲哚-4-酮制备

用间苯二酚在氢氧化钾参与下以镍催化氢化并异构化，生成3-酮基环己-1-烯醇钾，然后与溴代丙酮酸乙酯环合得4-氧代-4,5,6,7-四氢古马龙羧酸-3，进而以氨置换后者呋喃环上的氧并消除（脱羧）得到该品。

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1,5,6,7-四氢-4H-吲哚-4-酮海关

[ 海关编码 ]: 2933990090

[ 中文概述 ]:
2933990090. 其他仅含氮杂原子的杂环化合物. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:6.5%. 普通关税:20.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 乌洛托品请注明外观, 6－己内酰胺请注明外观, 签约日期

[ Summary ]:
2933990090. heterocyclic compounds with nitrogen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%

1,5,6,7-四氢-4H-吲哚-4-酮文献

Direct α-iodination of aryl alkyl ketones by elemental iodine activated by 1-chloromethyl-4-fluoro-1, 4-diazoniabicyclo [2.2. 2] octane bis (tetrafluoroborate). Jereb M, et al.

Synthesis 06 , 0853-0858, (2003)

DNA binders: 1. evaluation of DNA-interactive ability, design, and synthesis of novel intercalating agents Sechi M, et al.

Lett. Drug Des. Discov. 6(1) , 56-62, (2009)

Synthesis of pyrrolo [1, 2-a] indole-1, 8 (5H)-diones as new synthons for developing novel tricyclic compounds of pharmaceutical interest. Sechi M, et al.

ARKIVOC 5 , 97-106, (2004)

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