Synthesis and physiological activity of 1-(2-polyfluoroalkyl-1-iodoethyl) silatranes

MG Voronkov, VP Baryshok, EE Kuznetsova…

Index: Voronkov, M. G.; Baryshok, V. P.; Kuznetsova, E. E.; Remez, I. M.; Deev, L. E. Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 6 p. 405 - 409 Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 6 p. 44 - 47

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Abstract

The PMR spectra were run on a" Tesla BS487 C" spectrometer, using TMS as internal standard. The IR spectra were obtained on a" Specord IR" spectrophotometer in KBr tablets. l-(2'-Polyfluoroalkyl-l'-iodoethyl) silatranes (lX). A solution of i0 mmoles of 1-vinylsilatrane and 5.7-20 mmoles of the corresponding polyfluoroalkyl iodide was held in a sealed pyrex glass ampule witha scattered natural illumination, or was irradiated by hn7 light (a PRK-2 ...