Synthesis of Disulfides from the Palladium (0)-Catalyzed Reactions of Sulfenyl Halides and Organostannanes

JC Cochran, SR Friedman…

Index: Cochran, John C.; Friedman, Susan R.; Frazier, John P. Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536

Full Text: HTML

Citation Number: 11

Abstract

Palladium (0 or II)-catalyzed coupling reactions have acquired a well-established status in the synthetic organic repertoire. 1 A recent survey by Farina and coworkers2 revealed that a majority of the transition metalmediated cross-coupling reactions reported in 1992 involved palladium catalysis. While most examples involve the formation of carbon-carbon bonds, palladium-catalyzed formation of carbon-silicon, carbongermanium, and carbon-tin bonds ...

 Related Synthetic Route
N/A Structure

22024-99-3

N/A

~0%

o-nitrophenyl disulfide Structure

1155-00-6

o-nitrophenyl d...

Methyl bromide Structure

74-83-9

Methyl bromide

Methyl (2-nitrophenyl)sulfane Structure

3058-47-7

Methyl (2-nitro...

2,4,5-trichlorobenzenesulfenyl chloride Structure

62726-90-3

2,4,5-trichloro...

~0%

Bis(2,4,5-trichlorophenyl) Disulfide Structure

3808-87-5

Bis(2,4,5-trich...

2,4,5-Trichlorothioanisole Structure

4163-78-4

2,4,5-Trichloro...

2,4,5-trichlorobenzenesulfenyl chloride Structure

62726-90-3

2,4,5-trichloro...

Tetramethyltin Structure

594-27-4

Tetramethyltin

~%

Bis(2,4,5-trichlorophenyl) Disulfide Structure

3808-87-5

Bis(2,4,5-trich...

2,4,5-Trichlorothioanisole Structure

4163-78-4

2,4,5-Trichloro...

4-nitrobenzenesulfenyl chloride Structure

937-32-6

4-nitrobenzenes...

~0%

4-nitrophenyl methyl sulfide Structure

701-57-5

4-nitrophenyl m...

1,2-Bis(4-nitrophenyl)disulfane Structure

100-32-3

1,2-Bis(4-nitro...

2,4,5-trichlorobenzenesulfenyl chloride Structure

62726-90-3

2,4,5-trichloro...

~85%

Bis(2,4,5-trichlorophenyl) Disulfide Structure

3808-87-5

Bis(2,4,5-trich...

2,4,5-Trichlorothioanisole Structure

4163-78-4

2,4,5-Trichloro...

2,4,5-trichlorobenzenesulfenyl chloride Structure

62726-90-3

2,4,5-trichloro...

Tetramethyltin Structure

594-27-4

Tetramethyltin

~%

Bis(2,4,5-trichlorophenyl) Disulfide Structure

3808-87-5

Bis(2,4,5-trich...

2,4,5-Trichlorothioanisole Structure

4163-78-4

2,4,5-Trichloro...

Benzenesulfenylchloride, 2,4-dinitro- Structure

528-76-7

Benzenesulfenyl...

~0%

Disulfide,bis(2,4-dinitrophenyl) Structure

2217-55-2

Disulfide,bis(2...

Benzene,1-(methylthio)-2,4-dinitro- Structure

2363-23-7

Benzene,1-(meth...

Benzenesulfenylchloride, 2,4-dinitro- Structure

528-76-7

Benzenesulfenyl...

~0%

Chloromethane Structure

74-87-3

Chloromethane

Disulfide,bis(2,4-dinitrophenyl) Structure

2217-55-2

Disulfide,bis(2...

Benzene,1-(methylthio)-2,4-dinitro- Structure

2363-23-7

Benzene,1-(meth...

Tetramethyltin Structure

594-27-4

Tetramethyltin

Benzenesulfenylchloride, 2,4-dinitro- Structure

528-76-7

Benzenesulfenyl...

~%

Disulfide,bis(2,4-dinitrophenyl) Structure

2217-55-2

Disulfide,bis(2...

Benzene,1-(methylthio)-2,4-dinitro- Structure

2363-23-7

Benzene,1-(meth...

Benzenesulfenylchloride, 2,4-dinitro- Structure

528-76-7

Benzenesulfenyl...

~93%

Disulfide,bis(2,4-dinitrophenyl) Structure

2217-55-2

Disulfide,bis(2...

Benzene,1-(methylthio)-2,4-dinitro- Structure

2363-23-7

Benzene,1-(meth...

Benzenesulfenylchloride, 2,4-dinitro- Structure

528-76-7

Benzenesulfenyl...

~95%

Chloromethane Structure

74-87-3

Chloromethane

Disulfide,bis(2,4-dinitrophenyl) Structure

2217-55-2

Disulfide,bis(2...

Benzene,1-(methylthio)-2,4-dinitro- Structure

2363-23-7

Benzene,1-(meth...

o-nitrophenylsulfenyl chloride Structure

7669-54-7

o-nitrophenylsu...

~0%

o-nitrophenyl disulfide Structure

1155-00-6

o-nitrophenyl d...

Methyl (2-nitrophenyl)sulfane Structure

3058-47-7

Methyl (2-nitro...

N/A Structure

22024-99-3

N/A

~0%

o-nitrophenyl disulfide Structure

1155-00-6

o-nitrophenyl d...

Methyl bromide Structure

74-83-9

Methyl bromide

Methyl (2-nitrophenyl)sulfane Structure

3058-47-7

Methyl (2-nitro...

(chlorosulfanyl-diphenyl-methyl)benzene Structure

24165-03-5

(chlorosulfanyl...

~0%

[methylsulfanyl(diphenyl)methyl]benzene Structure

62575-83-1

[methylsulfanyl...

N/A Structure

15446-31-8

N/A

(chlorosulfanyl-diphenyl-methyl)benzene Structure

24165-03-5

(chlorosulfanyl...

Tetramethyltin Structure

594-27-4

Tetramethyltin

~%

[methylsulfanyl(diphenyl)methyl]benzene Structure

62575-83-1

[methylsulfanyl...

N/A Structure

15446-31-8

N/A

4-nitrobenzenesulfenyl chloride Structure

937-32-6

4-nitrobenzenes...

~84%

4-nitrophenyl methyl sulfide Structure

701-57-5

4-nitrophenyl m...

1,2-Bis(4-nitrophenyl)disulfane Structure

100-32-3

1,2-Bis(4-nitro...

o-nitrophenylsulfenyl chloride Structure

7669-54-7

o-nitrophenylsu...

~87%

o-nitrophenyl disulfide Structure

1155-00-6

o-nitrophenyl d...

Methyl (2-nitrophenyl)sulfane Structure

3058-47-7

Methyl (2-nitro...

N/A Structure

22024-99-3

N/A

~83%

o-nitrophenyl disulfide Structure

1155-00-6

o-nitrophenyl d...

Methyl bromide Structure

74-83-9

Methyl bromide

Methyl (2-nitrophenyl)sulfane Structure

3058-47-7

Methyl (2-nitro...


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