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1,2,3-三溴丙烷

1,2,3-三溴丙烷用途

用于杀线虫剂、溶剂、有机合成中间体。

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1,2,3-三溴丙烷名称

[ CAS 号 ]:
96-11-7

[ 中文名 ]:
1,2,3-三溴丙烷

[ 英文名 ]:
TRIBROMOHYDRIN

[中文别名 ]:

均三溴丙烷

[英文别名 ]:

Glycerol tribromohydrin
1,2,3-tribrompropane
Propane,1,2,3-tribromo
1,2,3-Tribromopropane
sym-Tribromopropane
1,2,3-tribromo propane
MFCD00017884
Glyceryl tribromohydrin
TRIBROMOHYDRIN
Allyl Tribromide

1,2,3-三溴丙烷物理化学性质

[ 密度 ]:
2.4±0.1 g/cm3

[ 沸点 ]:
220.5±8.0 °C at 760 mmHg

[ 熔点 ]:
16-17 °C(lit.)

[ 分子式 ]:
C₃H₅Br₃

[ 分子量 ]:
280.784

[ 闪点 ]:
87.7±13.2 °C

[ 精确质量 ]:
277.794128

[ LogP ]:
3.31

[ 外观性状 ]:
液体

[ 蒸汽压 ]:
0.2±0.4 mmHg at 25°C

[ 折射率 ]:
1.577

[ 储存条件 ]:
室温

1,2,3-三溴丙烷MSDS

1,2,3-三溴丙烷毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: TZ8300000

CHEMICAL NAME :: Propane, 1,2,3-tribromo-

CAS REGISTRY NUMBER :: 96-11-7

BEILSTEIN REFERENCE NO. :: 1732082

LAST UPDATED :: 199701

DATA ITEMS CITED :: 12

MOLECULAR FORMULA :: C3-H5-Br3

MOLECULAR WEIGHT :: 280.81

WISWESSER LINE NOTATION :: E1YE1E

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LDLo - Lowest published lethal dose

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 500 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :: Oral

DOSE :: 250 mg/kg

SEX/DURATION :: male 5 day(s) pre-mating

TOXIC EFFECTS :: Reproductive - Fertility - pre-implantation mortality (e.g. reduction in number of implants per female; total number of implants per corpora lutea) Reproductive - Fertility - post-implantation mortality (e.g. dead and/or resorbed implants per total number of implants) Reproductive - Fertility - litter size (e.g. # fetuses per litter; measured before birth)

TYPE OF TEST :: TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :: Intraperitoneal

DOSE :: 23869 ug/kg

SEX/DURATION :: male 1 day(s) pre-mating

TOXIC EFFECTS :: Reproductive - Paternal Effects - testes, epididymis, sperm duct Reproductive - Paternal Effects - other effects on male Reproductive - Specific Developmental Abnormalities - urogenital system

TYPE OF TEST :: DNA damage

MUTATION DATA

TEST SYSTEM :: Rodent - rat

DOSE/DURATION :: 250 mg/kg/5D (Continuous)

REFERENCE :: MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 101,321,1982 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - M1864 No. of Facilities: 8 (estimated) No. of Industries: 1 No. of Occupations: 6 No. of Employees: 176 (estimated)

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1,2,3-三溴丙烷安全信息

[ 符号 ]:

GHS07, GHS08

[ 信号词 ]:
Warning

[ 危害声明 ]:
H302 + H312 + H332-H315-H319-H335-H351

[ 警示性声明 ]:
P261-P280-P305 + P351 + P338

[ 个人防护装备 ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ 危害码 (欧洲) ]:
Xn:Harmful;

[ 风险声明 (欧洲) ]:
R20/21/22;R36/37/38;R68

[ 安全声明 (欧洲) ]:
S26-S27-S36/37/39

[ 危险品运输编码 ]:
2810

[ WGK德国 ]:
3

[ RTECS号 ]:
TZ8300000

[ 包装等级 ]:
II

[ 危险类别 ]:
6.1(b)

[ 海关编码 ]:
2903399090

1,2,3-三溴丙烷合成路线

1,2,3-三溴丙烷上下游产品

1,2,3-三溴丙烷上游产品

1,2,3-三溴丙烷下游产品

1,2,3-三溴丙烷制备

1.制法：

于装有搅拌器、回流冷凝器(装有氯化钙干燥管)、滴液漏斗、温度计的反应瓶中，加入烯丙基溴^①（2）182g(1.5mol),250mL干燥的四氯化碳。冰盐浴冷至-5℃，由滴液漏斗滴加干燥的溴255g(1.6mol),滴加速度控制在部使反应液升至0℃，约1.5h加完。慢慢升至室温并继续搅拌反应30min。减压蒸馏溶剂，而后收集92～93℃/1.33kpa的馏分，得几乎无色的液体1,2,3-三溴丙烷(1)400g，收率95%。注：①烯丙基溴在使用前最好进行处理，处理的方法如下：首先用无水氯化钙干燥，而后进行蒸馏，收集69～72℃的馏分。

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1,2,3-三溴丙烷海关

[ 海关编码 ]: 2903399090

[ 中文概述 ]:
2903399090. 其他无环烃的氟化、溴化或碘化衍生物. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:5.5%. 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途

[ Summary ]:
2903399090. brominated,fluorinated or iodinated derivatives of acyclic hydrocarbons. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:5.5%. General tariff:30.0%

1,2,3-三溴丙烷文献

Mutagenicity of halogenated propanes and their methylated derivatives.

Environ. Mol. Mutagen. 12(2) , 253-9, (1988)

1,2,3-Tribromopropane, 1,2,3-trichloropropane, and 1,2-dibromo-3-chloropropane are mutagenic in strains TA1535 and TA100 of Salmonella typhimurium, but only in the presence of rat liver S9 mix. This r...

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1,2,3-三溴丙烷

1,2,3-三溴丙烷用途

1,2,3-三溴丙烷名称

1,2,3-三溴丙烷物理化学性质

1,2,3-三溴丙烷MSDS

详细MSDS(安全技术说明书)

1,2,3-三溴丙烷毒性和生态

CHEMICAL IDENTIFICATION

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

MUTATION DATA

1,2,3-三溴丙烷安全信息

1,2,3-三溴丙烷合成路线

详细合成路线

1,2,3-三溴丙烷上下游产品

1,2,3-三溴丙烷上游产品

1,2,3-三溴丙烷下游产品

1,2,3-三溴丙烷制备

1,2,3-三溴丙烷海关

1,2,3-三溴丙烷文献

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